Cellulose derivatives with a low degree of substitution
Center for Innovative Technology
Virginia Polytechnic Institute and State University
Virginia Tech Intellectual Properties, Inc.
Glasser, Wolfgang G.
Samaranayake, Gamini S.
Sealey, II, James E.
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The invention is directed to the formation of cellulose derivatives using homogenous phase reaction conditions. Cellulose is dissolved using DMAc/LiCl and a reagent system is added to promote the acylation of an appropriate acid anhydride or free carboxylic acid. One reagent system includes N,N-dicyclohexylcarbodiimide (DCC) and 4-pyrrolidinopyridine (PP). Another reagent system includes p-toluene sulfonyl chloride (TsCl) and pyridine (Py).
- Virginia Tech Patents