Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry
dc.contributor.author | Whiton, R. S. | en |
dc.contributor.author | Zoecklein, Bruce W. | en |
dc.contributor.department | Food Science and Technology | en |
dc.date.accessed | 2014-07-09 | en |
dc.date.accessioned | 2014-07-10T13:56:43Z | en |
dc.date.available | 2014-07-10T13:56:43Z | en |
dc.date.issued | 2002 | en |
dc.description.abstract | A method for the rapid determination of ethyl carbamate in wine by headspace solid-phase microextraction with detection by gas chromatography/mass spectrometry has been developed. The analysis parameters of fiber coating, extraction time, and sample temperature have been optimized. The optimized method of headspace sampling with a Carbowax/divinylbenzene fiber for 30 minutes has been found to be reproducible and linear from 10 to 80 mug/L, with a limit of detection of 9.6 mug/L. The method is simple, requires little operator effort, and can be automated. | en |
dc.format.mimetype | application/pdf | en |
dc.identifier.citation | Whiton, R. S.; Zoecklein, B. W., "Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry," Am. J. Enol. Vitic 2002 vol. 53 no. 1 60-63. http://ajevonline.org/content/53/1/60.full | en |
dc.identifier.issn | 0002-9254 | en |
dc.identifier.uri | http://hdl.handle.net/10919/49446 | en |
dc.identifier.url | http://ajevonline.org/content/53/1/60.full | en |
dc.language.iso | en | en |
dc.publisher | American Society for Enology and Viticulture | en |
dc.rights | In Copyright | en |
dc.rights.uri | http://rightsstatements.org/vocab/InC/1.0/ | en |
dc.subject | ethyl carbamate | en |
dc.subject | solid-phase microextraction | en |
dc.subject | spme | en |
dc.subject | alcoholic beverages | en |
dc.subject | aroma compounds | en |
dc.subject | grape juice | en |
dc.subject | urea | en |
dc.subject | fermentation | en |
dc.subject | precursors | en |
dc.subject | ethanol | en |
dc.subject | biotechnology & applied microbiology | en |
dc.subject | food science & technology | en |
dc.subject | horticulture | en |
dc.title | Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry | en |
dc.title.serial | American Journal of Enology and Viticulture | en |
dc.type | Article - Refereed | en |
dc.type.dcmitype | Text | en |
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