Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry

dc.contributor.authorWhiton, R. S.en
dc.contributor.authorZoecklein, Bruce W.en
dc.contributor.departmentFood Science and Technologyen
dc.date.accessed2014-07-09en
dc.date.accessioned2014-07-10T13:56:43Zen
dc.date.available2014-07-10T13:56:43Zen
dc.date.issued2002en
dc.description.abstractA method for the rapid determination of ethyl carbamate in wine by headspace solid-phase microextraction with detection by gas chromatography/mass spectrometry has been developed. The analysis parameters of fiber coating, extraction time, and sample temperature have been optimized. The optimized method of headspace sampling with a Carbowax/divinylbenzene fiber for 30 minutes has been found to be reproducible and linear from 10 to 80 mug/L, with a limit of detection of 9.6 mug/L. The method is simple, requires little operator effort, and can be automated.en
dc.format.mimetypeapplication/pdfen
dc.identifier.citationWhiton, R. S.; Zoecklein, B. W., "Determination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometry," Am. J. Enol. Vitic 2002 vol. 53 no. 1 60-63. http://ajevonline.org/content/53/1/60.fullen
dc.identifier.issn0002-9254en
dc.identifier.urihttp://hdl.handle.net/10919/49446en
dc.identifier.urlhttp://ajevonline.org/content/53/1/60.fullen
dc.language.isoenen
dc.publisherAmerican Society for Enology and Viticultureen
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subjectethyl carbamateen
dc.subjectsolid-phase microextractionen
dc.subjectspmeen
dc.subjectalcoholic beveragesen
dc.subjectaroma compoundsen
dc.subjectgrape juiceen
dc.subjectureaen
dc.subjectfermentationen
dc.subjectprecursorsen
dc.subjectethanolen
dc.subjectbiotechnology & applied microbiologyen
dc.subjectfood science & technologyen
dc.subjecthorticultureen
dc.titleDetermination of ethyl carbamate in wine by solid-phase microextraction and gas chromatography/mass spectrometryen
dc.title.serialAmerican Journal of Enology and Viticultureen
dc.typeArticle - Refereeden
dc.type.dcmitypeTexten

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