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Sol-gel .beta.-aluminum titanate thin film coating

dc.contributor.assigneeCenter for Innovative Technologyen
dc.contributor.assigneeVirginia Polytechnic Institute and State Universityen
dc.contributor.inventorBrown, Nancy R.en
dc.contributor.inventorBrown, Jr., Jesse J.en
dc.contributor.inventorSun, Taweien
dc.date.accessed2016-08-19en
dc.date.accessioned2016-08-24T17:55:42Zen
dc.date.available2016-08-24T17:55:42Zen
dc.date.filed1993-07-28en
dc.date.issued1995-04-18en
dc.description.abstract.beta.-Al.sub.2 TiO.sub.5 protective coatings have been developed for both dense and porous ceramics such as SiC and Si.sub.3 N.sub.4 using a chemical solution processing method involving the hydrolysis and condensation of aluminum tri-sec butoxide and titanium butoxide. The solution viscosities, pH values, H.sub.2 O/alkoxide molar ratios, and dip coating withdrawal rates required for crack-free .beta.-Al.sub.2 TiO.sub.5 are 1.0 to 6.2 cP, pH 1-4.5, molar ratio 1.5-10, and withdrawal rate of 2.2-8.0 cm/min, respectively. Conversion of the amorphous coating to crystalline .beta.-Al.sub.2 TiO.sub.5 is achieved by a succession of calcination below 450.degree. C. and a final heat-treatment at 1300.degree. C. for ten hours with controlled heating and cooling rates.en
dc.format.mimetypeapplication/pdfen
dc.identifier.applicationnumber8098202en
dc.identifier.patentnumber5407479en
dc.identifier.urihttp://hdl.handle.net/10919/72832en
dc.identifier.urlhttp://pimg-fpiw.uspto.gov/fdd/79/074/054/0.pdfen
dc.language.isoen_USen
dc.publisherUnited States Patent and Trademark Officeen
dc.subject.cpcC01G23/003en
dc.subject.cpcC01P2006/22en
dc.subject.cpcC01P2006/32en
dc.subject.cpcC04B41/87en
dc.subject.cpcC04B35/478en
dc.subject.cpcC04B35/6264en
dc.subject.cpcC04B41/009en
dc.subject.cpcC04B41/5041en
dc.subject.cpcC04B41/4537en
dc.subject.cpcC04B41/4554en
dc.subject.cpcC04B41/463en
dc.subject.cpcC04B41/5016en
dc.subject.cpcC04B35/565en
dc.subject.cpcC04B35/584en
dc.subject.cpcC04B38/00en
dc.subject.cpcC04B2235/3206en
dc.subject.cpcC04B2235/441en
dc.subject.cpcC04B2235/443en
dc.subject.cpcC04B2235/656en
dc.subject.cpcC04B2235/6562en
dc.subject.cpcC04B2111/00112en
dc.subject.cpcC23C18/1216en
dc.subject.cpcC23C18/1254en
dc.subject.cpcC23C18/1283en
dc.subject.cpcC23C18/1295en
dc.subject.uspc106/287.19en
dc.subject.uspcother501/12en
dc.subject.uspcother516/77en
dc.subject.uspcother516/90en
dc.subject.uspcother516/93en
dc.subject.uspcother516/98en
dc.titleSol-gel .beta.-aluminum titanate thin film coatingen
dc.typePatenten
dc.type.dcmitypeTexten
dc.type.patenttypeutilityen

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