Comparison between beryllium and diamond-backing plates in diamond-anvil cells: Application to single-crystal x-ray diffraction high-pressure data

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dc.contributorVirginia Techen
dc.contributor.authorPeriotto, Benedettaen
dc.contributor.authorNestola, Fabrizioen
dc.contributor.authorBalic-Zunic, Toncien
dc.contributor.authorAngel, Ross J.en
dc.contributor.authorMiletich, Ronalden
dc.contributor.authorOlsen, Lars A.en
dc.contributor.departmentGeosciencesen
dc.date.accessed2014-01-25en
dc.date.accessioned2014-01-23T13:49:09Zen
dc.date.available2014-01-23T13:49:09Zen
dc.date.issued2011-05en
dc.description.abstractA direct comparison between two complete intensity datasets, collected on the same sample loaded in two identical diamond-anvil pressure cells equipped, respectively, with beryllium and diamond-backing plates was performed. The results clearly demonstrate that the use of diamond-backing plates significantly improves the quality of crystal structure data. There is a decrease in the internal R factor for averaging, structure refinement agreement factors, and in the errors and uncertainties of the atomic coordinates, atomic displacement parameters, and individual bond lengths. (C) 2011 American Institute of Physics. [doi:10.1063/1.3590776]en
dc.description.sponsorshipNational Science Foundation (NSF) EAR-0738692en
dc.description.sponsorshipDanish Agency for Science, Technology and Innovationen
dc.identifier.citationPeriotto, Benedetta; Nestola, Fabrizio; Balic-Zunic, Tonci; et al., "Comparison between beryllium and diamond-backing plates in diamond-anvil cells: Application to single-crystal x-ray diffraction high-pressure data," Rev. Sci. Instrum. 82, 055111 (2011); http://dx.doi.org/10.1063/1.3590776en
dc.identifier.doihttps://doi.org/10.1063/1.3590776en
dc.identifier.issn0034-6748en
dc.identifier.urihttp://hdl.handle.net/10919/25131en
dc.identifier.urlhttp://scitation.aip.org/content/aip/journal/rsi/82/5/10.1063/1.3590776en
dc.language.isoen_USen
dc.publisherAIP Publishingen
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subjectstructural evolutionen
dc.subjectsolid-solutionen
dc.subjectbehavioren
dc.subjectclinopyroxenesen
dc.titleComparison between beryllium and diamond-backing plates in diamond-anvil cells: Application to single-crystal x-ray diffraction high-pressure dataen
dc.title.serialReview of Scientific Instrumentsen
dc.typeArticle - Refereeden

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