Browsing by Author "Huxtable, Scott T."

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    Adsorption in Confined Aqueous Films
    Gaddam, Prudhvidhar Reddy (Virginia Tech, 2019-07-24)
    This thesis describes direct measurements of equilibrium adsorption of ions in thin (< 100 nm) aqueous films. Adsorption in thin films is important because it is through adsorption that the stability of colloidal suspensions is frequently tuned. The vast majority of measurements of adsorption to date have been to a single interfaces, whereas the subject of this thesis is adsorption in a thin film between two interfaces. There are two isolated interfaces when particles in a suspension are far apart, but during the collision, a thin film forms between the particles, and the properties of the thin film determines the stability of the colloid. Thus, adsorption in the thin film determines the stability of the colloidal dispersion. There is a distinct gap in the scientific literature concerning adsorption in thin films mainly because there is no technique for measuring such adsorption. To fill this gap in knowledge, I first developed of a technique to directly measure adsorption in thin films, and then applied this technique to explore the behavior of co-ions near charged interfaces as a function of bulk solution composition and the thickness of the film. The adsorption behavior of fluorescein, a di-anion, to negatively charged silica interfaces was studied in dilute electrolytes. The focus was on the effect of the electrostatic screening length, or Debye-length. The separation was measured using interference microscopy and the adsorption of fluorescein was measured using fluorescence microscopy. The Debye-length was altered by variation of the background salt (NaCl) concentration in dilute (<1 M) solution. The surface excess of adsorption for fluorescein was shown to depend on both the Debye-length and the separation distance between two interfaces. Increasing the Debye-length from 4 nm to 21 nm increased the plateau surface excess at large separations, and decreasing the separation lead to a monotonically decreasing surface excess. The surface excess varied over a range that scaled with the Debye-length. The results were compared to solution of the Poisson-Boltzmann model and good agreement was found between the model and the experiment. The effect of background salt concentration on fluorescein adsorption was also studied in concentrated electrolytes (2.5 – 10 M) for various monovalent salts (LiCl, NaCl and CsCl). The results showed that the fitted electrostatic screening length showed an opposite trend to predictions from Poisson-Boltzmann, with the screening-length increasing with increasing salt concentration. That is, the Debye-length prediction was quantitatively incorrect and predicts the incorrect trend. For example, in 10 M LiCl where the Debye-length is 0.1 nm, and therefore colloidal chemists would traditionally predict that double-layer forces are negligible, my results show that the actual decay length is about 10 nm, which is about the same as in 10-3 M LiCl solution. The rate of increase of screening-length as a function of concentration was also an ion specific effect. In addition, the results show that there is an inversion of the surface charge in concentrated salt solution. The original device on which all the above measurements were made had two limitations: (1) the maximum film thickness was 50 nm and (2) the film was asymmetric, which hampered calculation of the surface excess and increased the number of degrees of freedom in modeling of the adsorption. In the last part of my thesis, I describe development of a symmetric sample which (1) enables measurement of films up to 1 µm, (2) simplifies modeling of the optics by eliminating optical interference of the fluorescence excitation, and reduces the number of parameters when comparing to models.
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    Advanced Thermal Management Strategies – Scalable Coal-Graphene based TIMs and Additively Manufactured Heat Sinks
    Bharadwaj, Bharath Ramesh (Virginia Tech, 2022-06-27)
    With increased focus on miniaturization and high performance in electronics, thermal management is a very important area of research today. In multiple applications such as portable electronics, consumer electronics, military applications, automobile, power electronics, high performance computing, etc. innovative thermal management strategies are necessary. In this work, two novel approaches to dissipate redundant heat better- first by novel carbonaceous-nanoparticle additives to develop thermal interface materials with superior performance and the second by using advanced metal additive manufacturing techniques to design and analyze metal-lattice based heat sinks are presented. Thermal Interface Materials with multiple carbon-based nanoparticle fillers such as coal-derived Multi Layered Graphene (MLG), standard reduced Graphene Oxide (rGO), Multi-Walled Carbon Nano Tubes (MWCNTs), and Graphene Nano-Platelets (GNPs) in thermal paste were synthesized and seen to have superior heat dissipation properties. Also, graphene was synthesized from coal through an in-house, facile, scalable and cost-effective process. The enhancement in thermal conductance varies from ~70% in the coal-MLG to ~14% in MWCNTs-based TIMs. Noteworthy is ~3.5 times larger enhancement in thermal performance with the in-house coal-derived-MLG as compared to the commercially available g-MLG. At a 3% wt. fraction of coal-MLG, enhancement in thermal conductance was almost 120% higher compared to the base thermal grease. In the second part, metal lattice-based heat sinks are designed for additive manufacturing for use in passive cooling of high-flux thermal management. A parametric optimization based on the lattice geometry, thickness, and height subject to additive manufacturing constraints is conducted. Intricate metal lattices with low mass based on the Simple Cubic, Octet, and Voronoi structures were generated by implicit modelling in nTopology® and their thermal performance was analyzed through numerical analysis using commercial CFD packages. The Voronoi lattice performed best with a significant improvement in thermal performance (~18% reduction in junction temperature difference with respect to ambient) as compared to a standard baseline Longitudinal heat Sink (LHS), while reducing the mass of the heat sink by ~2.1 times. Such optimized metal lattice-based heat sinks can lead to significant downsizing, reduction in overall mass and cost in applications where thermal management is critical with a need for low mass. We believe that such novel scalable materials and processes suited for mass production could be critical in meeting the material, design and product development needs to tackle the thermal management challenges of the future.
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    Advances in Radiation Heat Transfer and Applied Optics, Including Application of Machine Learning
    Yarahmadi, Mehran (Virginia Tech, 2021-01-14)
    Artificial neural networks (ANNs) have been widely used in many engineering applications. This dissertation applies ANNs in the field of radiation heat transfer and applied optics. The topics of interest in this dissertation include both forward and inverse problems. Forward problems involve applications in which numerical simulation is expensive in terms of time consummation and resource utilization. Artificial neural networks can be applied in these problems for speeding up the process and reducing the required resources. The Monte Carlo ray-trace (MCRT) method is the state-of-the-art approach for modeling radiation heat transfer. It has the disadvantage of being a complex and computationally expensive process. In this dissertation, after first identifying the uncertainties associated with the MCRT method, artificial neural networks are proposed as an alternative whose computational cost is greatly reduced compared to traditional MCRT method. Inverse problems are concerned with situations in which the effects of a phenomenon are known but the cause is unknown. In such problems, available data in conjunction with ANNs provide an effective tool to derive an inverse model for recovering the cause of the phenomenon. Two problems are studied in this context. The first is concerned with an imager for which the readout power distribution is available and the viewed scene is of interest. Absorbed power distributions on a microbolometer array making up the imager is produced by discretized scenes using a high-fidelity Monte Carlo ray-trace model. The resulting readout array/scene pairs are then used to train an inverse ANN. It is demonstrated that a properly trained ANN can be utilized to convert the readout power distribution into an accurate image of the corresponding discretized scene. The recovered scene of the imager is helpful for monitoring the Earth's radiant energy budget. In the second problem, the collection of scattered radiation by a sun-photometer, or aureolemeter, is simulated using the MCRT method. The angular distribution of this radiation is summarized using the probability density function (PDF) of the incident angles on a detector. Atmospheric water cloud droplets are known to play an important role in determining the Earth's radiant energy budget and, by extension, the evolution of its climate. An extensive dataset is produced using an improved atmospheric scattering model. This dataset is then used to train and test an inverse ANN capable of recovering water cloud droplets properties from solar aureole observations.
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    Analysis of film cooling performance of tripod hole
    Ramesh, Sridharan (Virginia Tech, 2016-09-09)
    The thermal efficiency of a gas turbine directly depends on the rotor inlet temperature. The ever increasing demand for more power and advances in the field of engineering enabled this temperature to be pushed higher. But the material strength of the blades and vanes can often impose restrictions on the thermal load it can bear. This is where gas turbine cooling becomes very critical and a better cooling design has the potential to extend the blade life span, enables higher rotor inlet temperatures, conserves compressor bleed air. Among various kinds of cooling involved in gas turbines, film cooling will be the subject of this study. A novel concept for film cooling holes referred to as anti-vortex design proposed in 2007 is explored in this study. Coolant exits through two bifurcated cylindrical holes that branched out on either side of the central hole resulting in a tripod-like arrangement. Coolant from the side holes interacted with the mainstream and produced vortices that countered the main central rotating vortex pairs, weakening it and pushing the coolant jet towards the surface. In order to understand the performance of this anti-vortex tripod film cooling, a flat plate test setup and a low speed subsonic wind tunnel linear cascade were built. Transient heat transfer experiments were carried out in the flat plate test setup using Infrared thermography. Film cooling performance was quantified by measuring adiabatic effectiveness and heat transfer coefficient ratio. In order to gauge the performance, other standard hole geometries were also tested and compared with. Following the results from the flat plate test rig, film cooling performance was also evaluated on the surface of an airfoil. Adiabatic effectiveness was measured at different coolant mass flow rates. The tripod hole consistently provided better cooling compared to the standard cylindrical hole in both the flat plate and cascade experiments. In order to understand the anti-vortex concept which is one of the primary reason behind better performance of the tripod film cooling hole geometry, numerical simulations (CFD) were carried out at steady state using RANS turbulence models. The interaction of the coolant from the side holes with the mainstream forms vortices that tries to suppress the vortex formed by the central hole. This causes the coolant jet from the central to stay close to the surface and increases its coverage. Additionally, the coolant getting distributed into three individual units reduces the exit momentum ratio. Tripod holes were found to be capable of providing better effectiveness even while consuming almost half the coolant used by the standard cylindrical holes.
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    Application of Functional Safety Standards to the Electrification of a Vehicle Powertrain
    Neblett, Alexander Mark Hattier (Virginia Tech, 2018-08-02)
    With the introduction of electronic control units to automotive vehicles, system complexity has increased. With this change in complexity, new standards have been created to ensure safety at the system level for these vehicles. Furthermore, vehicles have become increasingly complex with the push for electrification of automotive vehicles, which has resulted in the creation of hybrid electric and battery electric vehicles. The goal of this thesis is to provide an example of a hazard and operability analysis as well as a hazard and risk analysis for a hybrid electric vehicle. Additionally, the safety standards developed do not align well with educational prototype vehicles because the standards are designed for corporations. The hybrid vehicle supervisory controller example within this thesis demonstrates how to define a system and then perform system-level analytical techniques to identify potential failures and associated requirements. Ultimately, through this analysis suggestions are made on how best to reduce system complexity and improve system safety of a student built prototype vehicle.
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    The Application of the Solar Chimney for Ventilating Buildings
    Park, David (Virginia Tech, 2016-11-09)
    This study sought to demonstrate the potential applications of the solar chimney for the naturally ventilating a building. Computational fluid dynamics (CFD) was used to model various room configurations to assess ventilation strategies. A parametric study of the solar chimney system was executed, and three-dimensional simulations were compared and validated with experiments. A new definition for the hydraulic diameter that incorporated the chimney geometry was developed to predict the flow regime in the solar chimney system. To mitigate the cost and effort to use experiments to analyze building energy, a mathematical approach was considered. A relationship between small- and full-scale models was investigated using non-dimensional analysis. Multiple parameters were involved in the mathematical model to predict the air velocity, where the predictions were in good agreement with experimental data as well as the numerical simulations from the present study. The second part of the study considered building design optimization to improve ventilation using air changes per hour (ACH) as a metric, and air circulation patterns within the building. An upper vent was introduced near the ceiling of the chimney system, which induced better air circulation by removing the warm air in the building. The study pursued to model a realistic scenario for the solar chimney system, where it investigated the effect of the vent sizes, insulation, and a reasonable solar chimney size. It was shown that it is critical to insulate the backside of the absorber and that the ratio of the conditioned area to chimney volume should be at least 10. Lastly, the application of the solar chimney system for basement ventilation was discussed. Appropriate vent locations in the basement were determined, where the best ventilation was achieved when the duct inlet was located near the ceiling and the exhaust vent was located near the floor of the chimney. Sufficient ventilation was also achieved even for scenarios of a congested building when modeling the presence of multiple people.
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    Artificial Anisotropy for Transverse Thermoelectric Heat Flux Sensing
    Derryberry, Rebekah Ann (Virginia Tech, 2007-04-05)
    Thermoelectric phenomenon describes the relationship between the flow of heat and electricity. Two main categories encompassed in thermoelectric theory are the Seebeck and Peltier effects. The Seebeck effect is the generation of a voltage in a device that consists of two different materials in the presence of a temperature gradient, while the Peltier effect is the generation of a temperature gradient across a device of two different materials in the presence of an electrical current. This project focuses on the first of these two phenomena, where the Seebeck effect is used in a novel heat flux sensor that is transverse in nature. Transverse thermoelectric devices are characterized by their anisotropy, meaning that a temperature gradient generated across a device will be perpendicular to the flow of electricity through the device. This orthogonal arrangement allows for the manipulation of material properties, device arrangement, and construction methods for device optimization. This project characterizes the heat flux sensing capabilities of an artificially anisotropic transverse thermoelectric device via experimental and theoretical methods. The device tested is constructed out of bismuth telluride and titanium grade 5. Bismuth telluride is a standard thermoelectric material, while the titanium is used because of its high melting point and good electrical conductivity. The device is constructed by alternating rectangular pieces of these two materials. These pieces are bonded together at a given angle to simulate anisotropy. Several devices are constructed in a range of angles from 59 to 88°. These devices are each tested in a vacuum chamber where a heater heats one side of the device. This heat flux into the device creates a temperature gradient across the device and the device generates a voltage perpendicular to this temperature gradient. Steady state data are collected for both the temperature difference between the two sides of the device and the voltage generated by the device. This procedure is repeated on each device for a range of heat fluxes from 0 to 2.6 W/cm². This range generates voltage signals up to 14341 µV for an angle of 59°. Data collected are then used to generate a linear trend line that describes the devices response to a given heat flux. These experimental results are compared to theoretical predictions using thermoelectric theory. The results indicate that the device does exhibit transverse thermoelectric characteristics and the experimental data follow the predicted trends. This thesis documents the process of constructing, testing, and analyzing this device.
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    Assessing Global Competence and Teamology for Collaborative Engineering
    Cobert, Matthew John (Virginia Tech, 2011-10-07)
    There is a need to make measureable improvements to the global competency of engineering students that will enable them to work more effectively with overseas colleagues. However, there are few assessment tools that offer clear guidance on which types of global exposure (coursework, virtual collaboration, or education abroad) provide substantial benefit. Additionally, with the increasing reliance on teams to solve problems in both industry and academia, there is a need to ensure high-performance and inventiveness. This thesis addresses these two challenges by 1) developing a new assessment tool for gauging global competency and evaluating a commercially-available tool, and 2) validating and simplifying Wilde's teamology method for assembling better teams. The newly developed Global Competence Survey (GCS) is a quick and effective tool that is able to delineate between student groups based upon duration of education abroad. In its current form, the GCS works by assessing student knowledge of key facts about USA and Germany, and their ability to recognize cultural images. This first attempt shows statistically significant differences between domestic, three-month abroad, and year-long abroad students in these critical areas. Additionally, the teamology method was confirmed empirically by analyzing the performance of two-person global research teams assembled using traditional selection criteria. This analysis shows that teams with greater personality diversity exhibit far higher performance and stronger cohesion. When coupled with functional role requirements, teamology provides an opportunity to dramatically enhance the team performance and cohesion of an available talent pool.
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    Assessment of Thermal Behavior and Development of Thermal Design Guidelines for Integrated Power Electronics Modules
    Pang, Ying-Feng (Virginia Tech, 2005-01-20)
    With the increase dependency on electricity to provide correct form of electricity for lightning, machines, and home and office appliances, the need for the introduction of high reliability power electronics in converting the raw form of electricity into efficient electricity for these applications is uprising. One of the most common failures in power electronics is temperature related failure such as overheating. To address the issue of overheating, thermal management becomes an important mission in the design of the power electronics to ensure the functional power electronics. Different approaches are taken by academia and industry researchers to provide efficient power electronics. In particular, the Center for Power Electronics System (CPES) at Virginia Tech and four other universities presented the IPEM approach by introducing integrated power electronics modules (IPEM) as standardized units that will enable greater integration within power electronics systems and their end-use application. The IPEM approach increases the integration in the components that make up a power electronics system through novel a packaging technique known as Embedded Power technology. While the thermal behavior of commonly used packages such as pin grid arrays (PGA), ball grid array (BGA), or quad flat pack (QFP) are well-studied, the influence of the Embedded Power packaging architecture on the overall thermal performance of the IPEMs is not well known. This motivates the presentation of this dissertation in developing an in-depth understanding on the thermal behavior of the Embedded Power modules. In addition, this dissertation outlines some general guidelines for the thermal modeling and thermal testing for the Embedded Power modules. Finally, this dissertation summarizes a few thermal design guidelines for the Embedded Power modules. Hence, this dissertation aims to present significant and generalized scientific findings for the Embedded Power packaging from the thermal perspective. Both numerical and experimental approaches were used in the studies. Three-dimensional mathematical modeling and computational fluid dynamics (CFD) thermal analyses were performed using commercial numerical software, I-DEAS. Experiments were conducted to validate the numerical models, characterize the thermal performance of the Embedded Power modules, and investigate various cooling strategies for the Embedded Power modules. Validated thermal models were used for various thermal analyses including identifying potential thermal problems, recognizing critical thermal design parameters, and exploring different integrated cooling strategies. This research quantifies various thermal design parameters such as the geometrical effect and the material properties on the thermal performance of the Embedded Power modules. These parameters include the chip-to-chip distance, the copper trace area, the polyimide thickness, and the ceramic materials. Since the Embedded Power technology utilizes metallization bonding as interconnection, specific design parameters such as the interconnect via holes pattern and size, the metallization thickness, as well as the metallization materials were also explored to achieve best results based on thermal and stress analyses. With identified potential thermal problems and critical thermal design parameters, different integrated cooling strategies were studied. The concept of integrated cooling is to incorporate the cooling mechanisms into the structure of Embedded Power modules. The results showed that simple structural modifications to the current Embedded Power modules can reduce the maximum temperature of the module by as much as 24%. Further improvement can be achieved by employing double-sided cooling to the Embedded Power modules. Based on the findings from the thermal analyses, general design guidelines were developed for future design of such Embedded Power modules. In addition, thermal modeling and testing guidelines for the Embedded Power modules were also outlined in this dissertation.
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    Augmentation of Jet Impingement Heat Transfer on a Grooved Surface Under Wet and Dry Conditions
    Alsaiari, Abdulmohsen Omar (Virginia Tech, 2018-11-27)
    Array jet impingement cooling experiments were performed on flat and grooved surfaces with the surface at a constant temperature. For the flat surface, power and temperature measurements were performed to obtain convection coefficients under a wide range of operating conditions such as jet speed, orifice to surface stand-of distance, and open area percentage. Cooling performance (CP) was calculated as the ratio between heat transfer and fan power. An empirical model was developed to predict jet impingement heat transfer taking into account the entrainment effects. Experimental results showed that jet impingement can provide high transfer rates with lower rates of cooling cost in comparison to contemporary conventional techniques in the industry. CP values over 279 were measured which are significantly higher than the standard values of 70 to 95 in current technology. The model enhanced prediction accuracy by taking into account the entrainment effects; an effect that is rarely considered in the literature. Experiments on the grooved surfaces were performed at dry and wet surface conditions. Under dry conditions, results showed 10%~55% improvement in heat transfer when compared to the flat surface. Improvement percentage tends to be higher at wider gaps between the array of orifices and the grooved surface. An improvement of 30%~40% was observed when increasing Re either by increasing orifice diameter or jet speed. Similar improvement was observed at higher flow open area percentages. No significant improvement in heat transfer resulted from decreasing the size of the grooves from 3.56mm to 2.54mm. Similarly, no noticeable change in heat transfer resulted from changing the relative position of the jets striking the surface at the top of the grooves to the bottom of the grooves. Deeper grooves with twice the depth gave statistically similar average heat transfer coefficients as shallower grooves. Under wet conditions, a hybrid cooling technique approach was proposed by using air jets impinging on a grooved surface with the grooves containing water. The approached is proposed and evaluated experimentally for its feasibility as an alternative for cooling towers of thermoelectric power plants. Convection heat and mass transfer coefficients were measured experimentally using the heat mass transfer analogy. Results showed that hybrid jet impingement provided high magnitudes of heat flux at low jet speeds and flow rates. High coefficients of performance CP > 3000, and heat fluxes > 8,000W/m2 were observed. Hybrid jet impingement showed 500% improvement as compared to jet impingement on a dry flat surface. CP values of hybrid jet impingement is 600% to 1,500% more as compared to performance of air-cooled condensers and wet cooling towers. Water use for hybrid jet impingement cooling is efficient since evaporation energy is absorbed from the surface directly instead of cooling air to near wet-bulb temperature.
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    Bench Scale Characterization of Joints and Coatings
    Kulkarni, Akhilesh (Virginia Tech, 2023-07-03)
    The ASTM E119 is a large-scale test used to qualify assemblies for fire resistance, including heat transmission and structural integrity. The test requires specialized furnaces and full-scale assemblies that are 3.0 m (10 ft) or more on each side, making it very expensive to perform. In this study, we investigated the feasibility of the scaling methodology for a reduced-scale fire resistance test on different types of wood-based structures, specifically commercially available intumescent coating applied onto wood and bolted lap joints in wood. We build upon a previously developed scaling methodology for wood and gypsum boards, which integrated geometric scaling, Fourier number time scaling, and furnace boundary condition matching. Intumescent coating presents a particular challenge in scaling in that it expands when exposed to fire conditions. To account for this expansion, we identified a relationship between initial dry film thickness and final expanded thickness through cone calorimeter tests and integrated it into a modified scaling methodology. This approach was then validated through fire exposure tests in furnace on wood samples painted with intumescent coating at full, half, and quarter scales. Finally, we demonstrated the scaling laws for joints under combined thermo-structural loading, by subjecting wood-based half-lap joint samples to combined bending and thermal loading at half and quarter scale. The samples were subjected to static three-point bending with the load scaled to achieve structural similitude, while simultaneously being exposed to a scaled fire exposure on the bottom surface. Our study provides insights into the practical application of scaling methodology for testing the fire resistance of joints and fire-resistant coated wood, paving the way for more cost-effective and quicker fire testing for the wood-based composite industry.
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    CFD analysis of airflow patterns and heat transfer in small, medium, and large structures
    Detaranto, Michael Francis (Virginia Tech, 2014-11-05)
    Designing buildings to use energy more efficiently can lead to lower energy costs, while maintaining comfort for occupants. Computational fluid dynamics (CFD) can be utilized to visualize and simulate expected flows in buildings and structures. CFD gives architects and designers the ability to calculate the velocity, pressure, and heat transfer within a building. Previous research has not modeled natural ventilation situations that challenge common design rules of thumb used for cross-ventilation and single-sided ventilation. The current study uses a commercial code (FLUENT) to simulate cross-ventilation in simple structures and analyzes the flow patterns and heat transfer in the rooms. In the Casa Giuliana apartment and the Affleck house, this study simulates passive cooling in spaces well-designed for natural ventilation. Heat loads, human models, and electronics are included in the apartment to expand on prior research into natural ventilation in a full-scale building. Two different cases were simulated. The first had a volume flow rate similar to the ambient conditions, while the second had a much lower flow rate that had an ACH of 5, near the minimum recommended value Passive cooling in the Affleck house is simulated and has an unorthodox ventilation method; a window in the floor that opens to an exterior basement is opened along with windows and doors of the main floor to create a pressure difference. In the Affleck house, two different combinations of window and door openings are simulated to model different scenarios. Temperature contours, flow patterns, and the air changes per hour (ACH) are explored to analyze the ventilation of these structures.
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    Characterization and Modeling of the Thermal Properties of Photopolymers for Material Jetting Processes
    Mikkelson, Emily Cleary (Virginia Tech, 2014-03-25)
    One emerging application of additive manufacturing is building parts with embedded electronics, but the thermal management of these assemblies is a potential issue. Electrical components have efficiency losses, and a significant portion of that lost energy is converted into heat. Embedding electronics in PolyJet parts is of particular interest since material jetting additive manufacturing has the ability to deposit multiple, functionally graded materials on a pixel by pixel basis. Although there is existing literature on other PolyJet material properties, there is limited research on their thermal characterization. The goal of this work is to determine the thermal conductivities of select PolyJet photopolymers (VeroWhitePlus, TangoBlackPlus, and Grey60) by using the heat flow meter method. The resulting thermal conductivities are then applied in finite element analysis (FEA) simulations to model the thermal distribution of heated PolyJet parts. Two FEA models of one-dimensional conduction in PolyJet parts are defined and compared to a corresponding physical model to verify the thermal conductivity measurements; one simulation expresses thermal conductivity as a function of temperature and the other uses an average value of thermal conductivity. The thermal conductivities were determined for a range of temperatures, and the average values were 0.2376 W/(m•K), 0.2307 W/(m•K), and 0.2272 W/(m•K) for VeroWhitePlus, TangoBlackPlus, and Grey60, respectively. When applying the thermal conductivity results to an FEA model, it was concluded that defining thermal conductivity as a function of temperature (as opposed to a constant value), reduced the average error in the predicted temperatures by less than 1%.
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    Comprehensive Modeling of Novel Thermal Systems: Investigation of Cascaded Thermoelectrics and Bio-Inspired Thermal Protection Systems Performance
    Kanimba, Eurydice (Virginia Tech, 2019-12-04)
    Thermal systems involve multiple components assembled to store or transfer heat for power, cooling, or insulation purpose, and this research focuses on modeling the performance of two novel thermal systems that are capable of functioning in environments subjected to high heat fluxes. The first investigated thermal system is a cascaded thermoelectric generator (TEG) that directly converts heat into electricity and offers a green option for renewable energy generation. The presented cascaded TEG allows harvesting energy in high temperatures ranging from 473K to 973K, and being a solid-state device with no moving parts constitutes an excellent feature for increase device life cycle and minimum maintenance in harsh, remote environments. Two cascaded TEG designs are analyzed in this research: the two-stage and three-stage cascaded TEGs, and based on the findings, the two-stage cascaded TEG produces a power output of 42 W with an efficiency of 8.3% while the three-cascaded TEG produces 51 W with an efficiency of 10.2%. The second investigated novel thermal system is a thermal protection system inspired by the porous internal skeleton of the cuttlefish also known as cuttlebone. The presented bio- inspired thermal protection has excellent features to serve as an integrated thermal protection system for spacecraft vehicles including being lightweight (93% porosity) and possessing high compressive strength. A large amount of heat flux is generated from friction between air and spacecraft vehicle exterior, especially during reentry into the atmosphere, and part of the herein presented research involves a thermomechanical modeling analysis of the cuttlebone bio-inspired integrated thermal protection system along with comparing its performance with three conventional structures such as the wavy, the pyramid, and cylindrical pin structures. The results suggest that the cuttlebone integrated thermal protection system excels the best at resisting deformation caused by thermal expansion when subjected to aerodynamic heat fluxes.
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    Computational and Experimental Modeling of the Bioheat Transfer Process of Perfusion in Tissue Applied to Burn Wounds
    Al-Khwaji, Abdusalam (Virginia Tech, 2013-04-29)
    A new mathematical model has been developed along with a new parameter estimation routine using surface temperature and heat flux measurements to estimate blood perfusion and thermal resistance in living tissue. Dynamic thermal measurements collected at the surface of the sensor before and after imposing a dynamic thermal cooling event are used with the model to estimate the blood perfusion, thermal resistance and core temperature. The Green\'s function based analytical solution does not require calculation of the whole tissue temperature distribution, which was not the case for the previous models. The result from the new model was proved to have better and more consistent results than previous models. The new model was validated to solve one of the unsolved biomedical problems which is the ability of detecting burn severity. The method was tested with a phantom perfusion system. The results matched known blood perfusion and thermal resistance values. The method was also tested with burns on animal models. Inflammation effects associated with the burns were studied using a newly developed term called the Burn Factor. This correlated with the severity of imposed burns. This work consists of three journal papers. The first paper introduces the mathematical model and its validation with finite-difference solutions. The second paper validates the physical aspects of the usage of the model with thermal measurement in detecting simulated burned layers and the associated perfusion. The third paper demonstrates the ability of the model to use thermal measurements to detect different burn severity of an animal model and to study the healing process.
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    Computational Study of Highway Bridges Structural Response Exposed to a Large Fire Exposure
    Nahid, Mohammad N. (Virginia Tech, 2015-07-08)
    The exposure from a localized vehicle fire has been observed to produce excessive damage onto highway bridge structural elements including complete collapse of the infrastructure. The occurrence of a fire beneath a bridge can lead to significant economic expense and loss of service even if the bridge does not collapse. The focus of the current research is to assess and evaluate the effect of realistic localized fire exposures from vehicles on the bridge structural integrity and to guide future development of highway bridge design with improved fire resistance. In this research, the bridge structural element response was predicted through a series of three loosely coupled analyses: fire analysis, thermal analysis, and structural analysis. Two different types of fire modeling methodologies were developed in this research and used to predict the thermo-structural response of bridge structural elements: one to model the non-uniform exposure due to a vehicle fire and another to predict response due to a standard uniform furnace exposure. The vehicle fire scenarios required coupling the computational fluid dynamics (CFD) code Fire Dynamics Simulator (FDS) with Abaqus while the furnace exposure scenarios were all done within Abaqus. Both methodologies were benchmarked against experimental data. Using the developed methodologies, simulations were initially performed to predict the thermo-structural response of a single steel girder-concrete deck composite assembly to different local, non-uniform fires and uniform standard furnace fire exposures. The steel girder-concrete deck composite assembly was selected since it is a common bridge design. Following this, a series of simulations were performed on unprotected highway bridges with multiple steel plate girders and steel tub girders subjected to localized fires. The analyses were used to evaluate the influence of a fire scenario on the bridge element response, identify the factors governing the failure of bridge structural elements subjected to a localized fire exposure, and provide guidance in the design of highway bridge structural elements against fire hazards. This study demonstrates that girder geometry affected both the dynamics of the fire as well as the heat transfer to the bridge structural elements which resulted in a different structural response for the bridge. A heavy goods vehicle (heat release rate of 200 MW) and tanker fires (heat release rate of 300 MW) were predicted to cause the bridge to fail due to collapse, while smaller fires did not. The geometric features of the plate girders caused the girder elements to be exposed to higher heat fluxes from both sides of the girder resulting in collapse when exposed to a HGV fire. Conversely, the closed feature of the box girder does not allow the interior surfaces to be in direct contact with the flames and are only exposed to the internal reradiation from surfaces inside the girder. As a result, the single and double lane tub girder highway bridge structure does not fail due to a heavy goods vehicle fire exposure.
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    Convection Calibration of Schmidt-Boelter Heat Flux Gages in Shear and Stagnation Air Flow
    Hoffie, Andreas Frank (Virginia Tech, 2006-12-19)
    This work reports the convection calibration of Schmidt-Boelter heat flux gages in shear and stagnation air flow. The gages were provided by Sandia National Laboratories and included two one-inch diameter and two one-and-one-half-inch diameter Schmidt-Boelter heat flux gages. In order to calibrate the sensors a convection calibration facility has been designed, including a shear test stand, a stagnation test stand, an air heater and a data acquisition system. The current physical model for a combined radiation and convection heat transfer environment uses an additional thermal resistance around the heat flux gage. This model clearly predicts a non-linear dependency of the gage sensitivity over a range of heat transfer coefficients. A major scope of this work was to experimentally verify the relation found by the model assumptions. Since the actual heat sink temperature is not known and cannot be measured, three different cases have been examined resulting in three different sensitivities for one pressure value, which is the gage sensitivity for the not cooled case and the gage sensitivity for the cooled case, based on the plate temperature or on the cooling water temperature. All of the measured sensitivities for shear as well as for stagnation flow fit well in the theory and show the non-linear decay for increasing heat transfer coefficient values. However, the obtained data shows an offset in the intersection with the sensitivity at zero heat transfer coefficient. This offset might arise from different radiation calibration techniques and different surface coatings of test gage and reference standard.
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    The Correlated Dynamics of Micron-Scale Cantilevers in a Viscous Fluid
    Robbins, Brian A. (Virginia Tech, 2014-12-08)
    A number of microcantilever systems of fundamental importance are explored using theoretical and numerical methods to quantify and provide physical insights into the dynamics of experimentally accessible systems that include a variety of configurations and viscous fluids. It is first shown that the correlated dynamics of both a laterally and vertically offset cantilever pair can be accurately predicted by numerical simulations. This is verified by comparing the correlated dynamics yielded by numerical simulations with experimental measurement. It is also demonstrated that in order to obtain these accurate predictions, geometric details of the cantilever must be included in the numerical simulation to directly reflect the experimental cantilever. A microrheology technique that utilizes the fluctuation-dissipation theorem is proposed. It is shown that by including the frequency dependence of the fluid damping, improvements in accuracy of the predictions of the rheological properties of the surrounding fluid are observed over current techniques. The amplitude spectrum of a 2-D cantilever in a power-law fluid is studied. The resulting amplitude spectrum yielded a curve similar to an overdamped system. It is observed that the amplitude and noise spectrum yield the same qualitative response for a 2-D cantilever in a shear thinning, power-law fluid. The correlated dynamics of a tethered vertically offset cantilever pair is investigated. It is shown that for a range of stiffness ratios, which is the ratio of the spring constant of the tethering relative to the cantilever spring constant, the change in the correlated dynamics of a Hookean spring tethered cantilever pair can be seen in the presence of fluid coupling. The dynamics of a spring-mass tethered, vertically offset cantilever pair is qualitatively studied by simplifying the model to an array of springs and masses. The resulting study found that the correlated dynamics of the displacement of mass of the tethered object yielded newly observed features and characteristics. It is shown that the curve shape of the cross-correlation of the displacement of the mass of the tethered object is similar to that of the auto-correlation of the displacement of the mass representing a step forced cantilever. The cross-correlation of the displacement of the mass of the tethered object, however, is found to be significantly more dependent on the stiffness ratio than the auto-correlation of the displacement of the mass representing a cantilever for t > 0. At t = 0, it is observed that the mass of the tethered object yields the same finite value for the cross-correlation for all studied values of the stiffness ratio. This characteristic is a result of the symmetry of the studied spring-mass system.
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    Correlation between structure, doping and performance of thermoelectric materials
    Zhao, Yu (Virginia Tech, 2014-09-08)
    Thermoelectric materials can convert thermal energy into electrical energy and vice-versa. They are widely used in energy harvesters, thermal sensors, and cooling systems. However, the low efficiency and high cost of the known material compositions limit their widespread utilization in electricity generation applications. Therefore, there is a strong interest in identifying new thermoelectric materials with high figure of merit. In response to this need, this dissertation works on the synthesis, structure, doping mechanism, and thermoelectric properties of zinc oxide (ZnO) and lead tellurium (PbTe). The main focus is on ZnO based materials and in improving their performance. The influences of micro- or nano-structures on thermal conductivity, as well as the correlation between the electrical property and synthesis conditions, have been systematically investigated. ZnO is a likely candidate for thermoelectric applications, because of its good Seebeck coefficient, high stability at high temperature, non-toxicity and abundance. Its main drawbacks are the high thermal conductivity (κ) and low electrical conductivity (σ). To decrease κ, two novel structures—namely, precipitate system and layered-and-correlated grain microstructure—have been proposed and synthesized in ZnO. The mechanisms iii governing the nature of thermal behavior in these structures have been explored and quantified. Due to strong phonon scattering, the nano-precipitates can reduce the thermal conductivity of ZnO by 73%. The ZnO with layered-and-correlated grains can further reduce κ by about 52%, which compares favorably with the dense ZnO with nanoprecipitates. The figure of merit of this ZnO based structure was 0.14×10⁻³ K⁻¹ at 573 K. In order to understand the electrical behavior in nanostructured ZnO, the impact of Al doping and chemical defects in ZnO under different synthesis conditions were studied. Under varying sintering temperatures, atmospheres and initial physical conditions, ZnO exhibited very distinct σ. High temperature, lack of oxygen, vacuum condition, and chemically synthesized powder can increase the carrier concentration and σ of ZnO. A promising alloy system, PbTe-PbS, undergoes natural phase separation by nucleation and growth, and spinodal decomposition depending on the thermal treatment. The correlation between the thermal treatment, structure, and the thermoelectric properties of Pb0.9S0.1Te has been studied. The nano-precipitates were incorporated in the annealed alloy resulting in a 40% decrease in κ. The PbS precipitation was shown to enhance the carrier concentration and improves the Seebeck coefficient. These concomitant effects result in a maximum ZT of 0.76 at 573 K. Throughout the thesis, the emphasis was on understanding the impact of the microstructures on thermal conductivity and the effect of the synthesis condition on thermal and electrical properties. The process and control variables identified in this study provide practical ways to optimize the figure of merit of ZnO and PbTe materials for thermoelectric applications.
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    Creating Complex Hollow Metal Geometries Using Additive Manufacturing and Metal Plating
    McCarthy, David Lee (Virginia Tech, 2012-06-25)
    Additive manufacturing introduces a new design paradigm that allows the fabrication of geometrically complex parts that cannot be produced by traditional manufacturing and assembly methods. Using a cellular heat exchanger as a motivational example, this thesis investigates the creation of a hybrid manufacturing approach that combines selective laser sintering with an electroforming process to produce complex, hollow, metal geometries. The developed process uses electroless nickel plating on laser sintered parts that then undergo a flash burnout procedure to remove the polymer, leaving a complex, hollow, metal part. The resulting geometries cannot be produced directly with other additive manufacturing systems. Copper electroplating and electroless nickel plating are investigated as metal coating methods. Several parametric parts are tested while developing a manufacturing process. Copper electroplating is determined to be too dependent on the geometry of the part, with large changes in plate thickness between the exterior and interior of the tested parts. Even in relatively basic cellular structures, electroplating does not plate the interior of the part. Two phases of electroless nickel plating combined with a flash burnout procedure produce the desired geometry. The tested part has a density of 3.16g/cm3 and withstands pressures up to 25MPa. The cellular part produced has a nickel plate thickness of 800µm and consists of 35% nickel and 65% air (empty space). Detailed procedures are included for the electroplating and electroless plating processes developed.