Microbore HPLC methodology and temperature programmed microbore HPLC

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dc.contributor.authorBowermaster, Jeffreyen
dc.contributor.committeechairMcNair, Harold M.en
dc.contributor.committeememberDillard, John G.en
dc.contributor.committeememberField, Paul E.en
dc.contributor.committeememberMason, John G.en
dc.contributor.committeememberTaylor, Larry T.en
dc.contributor.departmentChemistryen
dc.date.accessioned2017-03-10T15:14:59Zen
dc.date.available2017-03-10T15:14:59Zen
dc.date.issued1984en
dc.description.abstractSmall diameter LC columns provide rapid thermal equilibration and are ideal candidates for temperature programmed LC. Special instrumentation requirements are presented and details of column assembly are given to permit the preparation of highly efficient, stable microbore columns. Three LC temperature control systems are described and their individual strengths and weaknesses are discussed. Problems encountered in raising the temperature of an LC column are addressed and solutions are described. Experimental results of column and instrumentation evaluation are given and the effects of temperature on speed, efficiency, stability and retention of a broad range of samples is reported. Temperature and solvent programming are compared directly.en
dc.description.degreePh. D.en
dc.format.extentxiv, 239 leavesen
dc.format.mimetypeapplication/pdfen
dc.identifier.urihttp://hdl.handle.net/10919/76059en
dc.language.isoen_USen
dc.publisherVirginia Polytechnic Institute and State Universityen
dc.relation.isformatofOCLC# 12491804en
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subject.lccLD5655.V856 1984.B682en
dc.subject.lcshHigh performance liquid chromatographyen
dc.titleMicrobore HPLC methodology and temperature programmed microbore HPLCen
dc.typeDissertationen
dc.type.dcmitypeTexten
thesis.degree.disciplineChemistryen
thesis.degree.grantorVirginia Polytechnic Institute and State Universityen
thesis.degree.leveldoctoralen
thesis.degree.namePh. D.en

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