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Structural studies of precursor and partially oxidized conducting complexes. II. A neutron diffraction study of disodium dibromotetracyanoplatinate dihydrate

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dc.contributor.authorMaffly, Robert L.en
dc.contributor.authorJohnson, Paul L.en
dc.contributor.authorKoch, Timothy R.en
dc.contributor.authorWilliams, Jack M.en
dc.date.accessioned2022-08-17T19:47:15Zen
dc.date.available2022-08-17T19:47:15Zen
dc.date.issued1977-02-01en
dc.date.updated2022-08-06T22:26:45Zen
dc.description.abstractNa<sub>2</sub>[Pt(CN)<sub>4</sub>Br<sub>2</sub>]. 2H<sub>2</sub>O, orthorhombic, Pnma (D<sub>2h</sub><sup>16</sup>), a = 11.949(11), b = 15.124(14), c = 6.487 (6) Å, Z = 4, D<sub>m</sub> = 3.06, D<sub>x</sub> = 3.065 g cm<sup>-3</sup>. A room-temperature, single-crystal neutron diffraction study was performed. The structure was solved by direct methods and refined by full-matrix least-squares techniques to R(F<sub>0</sub><sup>2</sup>) = 0.068 for 1447 observed reflections > 1σ(F<sub>0</sub><sup>2</sup>). The structure consists of octahedrally coordinated platinum (IV) complex anions interacting with both the sodium cations and the waters of hydration.en
dc.description.versionPublished versionen
dc.format.extentPages 558-560en
dc.format.mimetypeapplication/pdfen
dc.identifier.doihttps://doi.org/10.1107/s0567740877004075en
dc.identifier.issn0567-7408en
dc.identifier.issue2en
dc.identifier.orcidKoch, Timothy [0000-0002-8026-9653]en
dc.identifier.urihttp://hdl.handle.net/10919/111542en
dc.identifier.volume33en
dc.language.isoenen
dc.publisherInternational Union of Crystallographyen
dc.rightsPublic Domain (U.S.)en
dc.rights.urihttp://creativecommons.org/publicdomain/mark/1.0/en
dc.titleStructural studies of precursor and partially oxidized conducting complexes. II. A neutron diffraction study of disodium dibromotetracyanoplatinate dihydrateen
dc.title.serialActa Crystallographica Section B Structural Crystallography and Crystal Chemistryen
dc.typeArticle - Refereeden
dc.type.dcmitypeTexten
pubs.organisational-group/Virginia Techen
pubs.organisational-group/Virginia Tech/VT Carilion School of Medicineen
pubs.organisational-group/Virginia Tech/VT Carilion School of Medicine/Internal Medicineen
pubs.organisational-group/Virginia Tech/VT Carilion School of Medicine/Internal Medicine/General IMen

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