Heat transfer and scale resisting properties of silicone resins

dc.contributor.authorGriffith, Andrewen
dc.contributor.departmentChemical Engineeringen
dc.date.accessioned2017-03-09T21:34:52Zen
dc.date.available2017-03-09T21:34:52Zen
dc.date.issued1947en
dc.description.abstractThe effects of silicone coated heat-exchanger tubes on the water film coefficient of heat transfer and on the formation of gypsum seals were studied. The heat-exchanger tubes consisted of 74 ½-in. sections of 1-in. Nominal diameter standard iron pipe into whose surface were installed six copper-constantan thermocouples for measuring the temperature of the tube well. Silicone resins DC 804 and DC 802 were used for coating the tubes. Silicone resin DC 804 was cured for 16 hours under infra-red heat at 440-450°F to a pencil hardness of 7H; however, due to the fact that it would not withstand the thermal stresses encountered in the heat-exchanger, its use was abandoned. Silicone resin DC 802 was cured for 12 hours under infra-red heat at 440-450°F to a pencil hardness of 2H. The horizontal tube double-pipe heat-exchanger consisted of a 5-ft. section of 2-in. I.D. Pyrex pipe fitted with a reducing tee and a reducing cross as the end-sections. Heat was applied to the heat-exchanger by steam from 15 to 40 psig. In the "Heat Transfer Tests", which were conducted with water at 60°F and at Reynolds numbers from 2500 to 11,000, it was found that the water film coefficients on the silicon surface varied from 810 to 1590 BTu/(hr.)(sq.ft.)(°F); while those on non-coated iron tubes varied from 244 to 670 under the same conditions. In "Accelerated scaling tests", which were conducted at Reynolds numbers of 15,000 and 4,100 using a saturated gypsum solution at l55°F as the scaling medium, it was found that scale formation on the coated and non-coated tubes reduced the film coefficient approximately 50 percent in 3 ½ to 4 ½ hours. A coating of 0.0006-in. Thickness caused the initial water film coefficient to be 70 percent of the coefficient for a non-coated tube at a Reynolds number of 15,000. A coating of 0.0018-in. thickness caused the initial. water film coefficient to be 83 per eent of the initial coefficient for a non-coated tube at a Reynolds number of 4,100. The thermal conductivity of silicone resin DC 802 was found to be 0.096-0.103 Btu/(hr.)(aq.ft.)(°F per ft.) at 150°F.en
dc.description.degreeMaster of Scienceen
dc.format.extent135 leavesen
dc.format.mimetypeapplication/pdfen
dc.identifier.urihttp://hdl.handle.net/10919/75957en
dc.language.isoen_USen
dc.publisherVirginia Polytechnic Instituteen
dc.relation.isformatofOCLC# 28315663en
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subject.lccLD5655.V855 1947.G754en
dc.subject.lcshSilicon resinen
dc.subject.lcshGums and resinsen
dc.titleHeat transfer and scale resisting properties of silicone resinsen
dc.typeThesisen
dc.type.dcmitypeTexten
thesis.degree.disciplineChemical Engineeringen
thesis.degree.grantorVirginia Polytechnic Instituteen
thesis.degree.levelmastersen
thesis.degree.nameMaster of Scienceen

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