A synthesis of dibenzo (a,e) perylene

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dc.contributor.authorPavlik, James Williamen
dc.contributor.committeechairVingiello, Frank A.en
dc.contributor.departmentChemistryen
dc.date.accessioned2014-03-14T21:37:37Zen
dc.date.adate2012-06-10en
dc.date.available2014-03-14T21:37:37Zen
dc.date.issued1961-07-05en
dc.date.rdate2012-06-10en
dc.date.sdate2012-06-10en
dc.description.abstractThe ayelodehydrogenation of 7-(1-naphthyl)benz [a] anthracene to dibenzo [a,e] perylene was accomplished in 38% yield using an aluminum chloride - stannic chloride catalyst. Attempts to reproduce or to improve this yield were not successful and thereafter the only product isolated was a low melting light orange solid which was postulated to be a hydrogenated intermediate. That the orange material could be converted to dibenzo [a,e] perylene upon treatment with palladiem on charcoal in p-eymene substantiated this postulation.en
dc.description.degreeMaster of Scienceen
dc.format.extent59 leavesen
dc.format.mediumBTDen
dc.format.mimetypeapplication/pdfen
dc.identifier.otheretd-06102012-040101en
dc.identifier.sourceurlhttp://scholar.lib.vt.edu/theses/available/etd-06102012-040101/en
dc.identifier.urihttp://hdl.handle.net/10919/43027en
dc.language.isoenen
dc.publisherVirginia Techen
dc.relation.haspartLD5655.V855_1961.P384.pdfen
dc.relation.isformatofOCLC# 22537077en
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subject.lccLD5655.V855 1961.P384en
dc.subject.lcshBenzanthracenes -- Researchen
dc.subject.lcshDehydrogenation -- Researchen
dc.subject.lcshPerylene -- Synthesisen
dc.titleA synthesis of dibenzo (a,e) peryleneen
dc.typeThesisen
dc.type.dcmitypeTexten
thesis.degree.disciplineChemistryen
thesis.degree.grantorVirginia Polytechnic Instituteen
thesis.degree.levelmastersen
thesis.degree.nameMaster of Scienceen

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