Retention trends of chemical classes using CCl₄ as a carrier solvent in normal-phase HPLC
dc.contributor.author | Wang, Muh S. | en |
dc.contributor.department | Chemistry | en |
dc.date.accessioned | 2021-10-26T20:09:59Z | en |
dc.date.available | 2021-10-26T20:09:59Z | en |
dc.date.issued | 1985 | en |
dc.description.abstract | Carbon tetrachloride (CCl₄ ) was closely evaluated as a carrier solvent in high-performance liquid chromatography (HPLC). The separation and retention trends of ninety-two selected compounds from eleven chemical classes (furans, thiophenes, aromatic hydrocarbons, ethers, esters, ketones, aldehydes, aromatic amines, azaarenes, alcohols and phenols) on three analytical silica-bonded phase (amino (NH₂), cyano (CN) and polar amino-cyano (PAC)) columns were investigated with CCl₄ and refractive index (RI) detection. The sample capacity and column efficiency of each of the NH₂ and PAC columns were measured and compared. Besides, a method of determining unmeasurable capacity factors (k' values) was found and illustrated. | en |
dc.description.degree | M.S. | en |
dc.format.extent | v, 69 leaves | en |
dc.format.mimetype | application/pdf | en |
dc.identifier.uri | http://hdl.handle.net/10919/106063 | en |
dc.language.iso | en | en |
dc.publisher | Virginia Polytechnic Institute and State University | en |
dc.relation.isformatof | OCLC# 13047077 | en |
dc.rights | In Copyright | en |
dc.rights.uri | http://rightsstatements.org/vocab/InC/1.0/ | en |
dc.subject.lcc | LD5655.V855 1985.W362 | en |
dc.subject.lcsh | Carbon tetrachloride | en |
dc.subject.lcsh | High performance liquid chromatography | en |
dc.title | Retention trends of chemical classes using CCl₄ as a carrier solvent in normal-phase HPLC | en |
dc.type | Thesis | en |
dc.type.dcmitype | Text | en |
thesis.degree.discipline | Chemistry | en |
thesis.degree.grantor | Virginia Polytechnic Institute and State University | en |
thesis.degree.level | masters | en |
thesis.degree.name | M.S. | en |
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