Flotation of Extreme Particle Sizes

dc.contributor.authorLeland, Jack Hambletonen
dc.contributor.committeechairYoon, Roe H.en
dc.contributor.committeememberGupta, Mohiten
dc.contributor.committeememberQiao, Ruien
dc.contributor.departmentMechanical Engineeringen
dc.date.accessioned2026-03-24T08:00:10Zen
dc.date.available2026-03-24T08:00:10Zen
dc.date.issued2026-03-23en
dc.description.abstractFlotation is effective over a narrow particle size range. As particle sizes increase above ~150 µm, body detachment forces overcome surface attachment forces, while, at the same time, mineral liberation decreases, reducing attachment force increasing the detachment probability. As particle sizes decrease below ~20 µm, the collision probabilities between bubbles and particles decrease because fine particles follow streamlines around bubbles due to their low inertia. In this work, Jig Flotation and Two Liquid Flotation (TLF) are developed to extend the maximum and minimum particle size of flotation, respectively. The Jig Flotation process reduces detachment probabilities using an intermittent fluidized bed instead of a mechanically agitated flotation cell for bubble-particle collision. The pulsion and suction cycles creating the intermittent fluidization allow for the formation of a froth phase, allowing Jig Flotation to be selective for both fine and coarse particles. The jigging mechanism allows particles to be separated by density independent of particle size. This mechanism is enabled by the attachment of bubbles to selectively hydrophobized minerals, reducing their apparent density and enhancing their density difference with gangue minerals. In the present work, several Jig Flotation cells have been designed and tested, and encouraging results achieved on chalcopyrite ore. The TLF process uses recyclable oils instead of air bubbles to recover ultrafine coal particles. Oil, having higher contact angles than air bubbles, enhances the recovery of ultrafine particles. The TLF process has produced coal with below 5% ash and below 2% moisture with recoveries greater than 80% from fine coal wastes.en
dc.description.abstractgeneralFlotation is effective for only some particle sizes. As particle sizes increase above ~150 µm, particles are more likely to detach from bubbles due to their lower area of exposed minerals. As particle sizes decrease below ~20 µm, particles tend to flow around bubbles due to their low mass, making them more difficult to recover. In this work, Jig Flotation and Two Liquid Flotation (TLF) are developed to overcome the challenges for small and large particles, respectively. The Jig Flotation process reduces detachment probabilities using an alternately upward and downward flow of fluid instead of mixing as used in traditional flotation cells for bubble-particle collision. The alternating upward and downward flow allows froth to collect at the top of the cell, keeping unwanted fine particles from being recovered. The jigging mechanism allows particles to be separated by density independent of particle size. This mechanism is enabled by the attachment of bubbles to selectively the desired particles, reducing their apparent density and enhancing their density difference with undesired minerals. In the present work, several Jig Flotation cells have been designed and tested, and encouraging results achieved on copper ore. The TLF process uses recyclable oils instead of air bubbles to recover small coal particles. Oil attracts and attaches to target particles more strongly than air bubbles, enhancing the recovery of small particles. The TLF process has produced coal with below 5% impurity and below 2% moisture with recoveries greater than 80% from fine coal wastes.en
dc.description.degreeMaster of Scienceen
dc.format.mediumETDen
dc.identifier.othervt_gsexam:45758en
dc.identifier.urihttps://hdl.handle.net/10919/142407en
dc.language.isoenen
dc.publisherVirginia Techen
dc.rightsIn Copyrighten
dc.rights.urihttp://rightsstatements.org/vocab/InC/1.0/en
dc.subjectFlotationen
dc.subjectCoarse Particle Flotationen
dc.subjectUltrafine Particlesen
dc.subjectDewateringen
dc.subjectCoal Wasteen
dc.subjectChalcopyriteen
dc.titleFlotation of Extreme Particle Sizesen
dc.typeThesisen
thesis.degree.disciplineMechanical Engineeringen
thesis.degree.grantorVirginia Polytechnic Institute and State Universityen
thesis.degree.levelmastersen
thesis.degree.nameMaster of Scienceen

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